Category: 99-61-6

In 2021 DALTON T published article about CATALYZED OXIDATIVE SYNTHESIS; ONE-POT SYNTHESIS; 4(3H)-QUINAZOLINONE DERIVATIVES; CASCADE SYNTHESIS; BENZYL ALCOHOLS; QUINAZOLINONES; METAL; EFFICIENT; SILICA; OXIDE in [Gupta, Radhika; Arora, Gunjan; Yadav, Priya; Dixit, Ranjana; Sharma, Rakesh Kumar] Univ Delhi, Green Chem Network Ctr, Dept Chem, Delhi 110007, India; [Yadav, Priya; Srivastava, Anju] Univ Delhi, Hindu Coll, Dept Chem, Delhi 110007, India in 2021, Cited 74. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6. SDS of cas: 99-61-6

In the present work, we report the design and fabrication of a copper-containing ionic liquid supported magnetic nanocatalyst via a convenient and straightforward synthetic approach for the formation of 2-phenylquinazolin-4(3H)-ones using o-aminobenzamide and benzaldehydes as the reaction partners. The successful formation and properties of the as-prepared catalyst have been thoroughly investigated using diverse physico-chemical techniques including FT-IR, XRD, FE-SEM, TEM, ICP, VSM, BET and TGA. Using this nanocatalytic system, a variety of 2-phenylquinazolin-4(3H)-ones are synthesized in excellent yields with operational ease and short reaction times in an environmentally preferable solvent under open air and without using any external oxidizing agent. Besides, the catalyst possessed facile magnetic recoverability and remarkable reusability for six consecutive runs without any appreciable decrease in the catalytic efficiency.

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Reference:
Thiomorpholine – Wikipedia,
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I found the field of Chemistry very interesting. Saw the article Highly efficacious preparation of 3,3 ‘-(arylmethylene)-bis(2-hydroxynaphthoquinone) derivatives catalyzed by a nanorod-structured organic-inorganic hybrid material published in 2021. Quality Control of 3-Nitrobenzaldehyde, Reprint Addresses Zare, A (corresponding author), Payame Noor Univ, Dept Chem, POB 19395-3697, Tehran, Iran.. The CAS is 99-61-6. Through research, I have a further understanding and discovery of 3-Nitrobenzaldehyde

A nanorod-structured organic-inorganic hybrid material namely nanorod-[SiO2-Pr-Im-SO3H][CF3CO2] (N-[SPIS][TFA]) has been applied as a highly efficacious, dual-functional, and recoverable catalyst for the solvent-free preparation of 3,3′-(arylmethylene)-bis(2-hydroxynaphthoquinone) {3,3 ‘-(arylmethylene)-bis(2-hydroxynaphthalene-1,4-dione)} derivatives in high yields and relatively short times. The one-pot pseudo-multi-component reaction of 2-hydroxynaphthoquinone (2-hydroxynaphthalene-1,4-dione) (2 eq.) and arylaldehydes (1 eq.) has been used for the preparation of these compounds. [GRAPHICS]

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Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

In 2021.0 J PEPT SCI published article about ARTIFICIAL METALLOENZYMES; ASYMMETRIC HYDROGENATION; PEPTIDES; COMPLEXES; 8-AMINO-5,6,7,8-TETRAHYDROQUINOLINE; KETONES in [Rimoldi, Isabella; Bucci, Raffaella; Feni, Lucia; Facchetti, Giorgio; Pellegrino, Sara] Univ Milan, Dipartimento Sci Farmaceut, Via Venezian 21, I-20133 Milan, Italy; [Santagostini, Laura] Univ Milan, Dipartimento Chim, Milan, Italy in 2021.0, Cited 48.0. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6. Quality Control of 3-Nitrobenzaldehyde

Mets7is a methionine-rich motif present in hCtr-1 transporter that is involved in copper cellular trafficking. Its ability to bind Cu(I) was recently exploited to develop metallopeptide catalysts for Henry condensation. Here, the catalytic activity ofMets7-Cu(I)complex in Michael addition reactions has been evaluated. Furthermore,His7peptide, in which Met residues have been substituted with His ones, was also prepared. This substitution allowedHis7to coordinate Cu (II), with the obtainment of a stable turn conformation as evicted by CD experiments.His7-Cu (II)proved also to be a better catalyst thanMets7-Cu(I)in the addition reaction. In particular, when the substrate was the (E)-1-phenyl-3-(pyridin-2-yl)prop-2-en-1-one, a conversion of 71% and a significative 58% of e.e. was observed.

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Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

Authors Gong, K; Zhang, DQ; Wang, YY; Li, CH; Zhang, HM; Li, HR; Feng, HR in ELSEVIER published article about KNOEVENAGEL CONDENSATION; MICHAEL ADDITION; HIGHLY EFFICIENT; IONIC LIQUIDS; MALONONITRILE; ALDEHYDES; NANOPARTICLES; NANOCATALYST; DIOXIDE in [Gong, Kai; Zhang, Daquan; Wang, Yunyun; Li, Cunhao; Zhang, Huimin; Li, Haoran; Feng, Huiru] Jiangnan Univ, Sch Pharmaceut Sci, Wuxi 214122, Jiangsu, Peoples R China in 2021.0, Cited 51.0. SDS of cas: 99-61-6. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6

Covalent organic frameworks (COFs) can be rationally designed with desired physicochemical properties for a far-ranging application in catalytic systems. Herein, a biguanide-functionalized covalent organic framework was designed and prepared via N-alkylation reaction, exhibiting a granular aggregate structure with high specific surface area. The biguanide-decorated DG-COF can be used as a highly efficient basic catalyst for the Knoevenagel condensation and Knoevenagel-Michael-cyclocondensation reaction. The present methodology is of excellent yields, short reaction times and simple operational procedure. DG-COF catalytic performance does not change after eight-times regeneration.

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Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

An article Selective oxidation of benzyl alcohols to benzaldehydes catalyzed by dioxomolybdenum Schiff base complex: synthesis, spectral characterization, crystal structure, theoretical and computational studies WOS:000647974300001 published article about SOLVENT-FREE; SPECTROSCOPIC CHARACTERIZATION; METAL-COMPLEXES; EPOXIDATION; MONONUCLEAR in [Kargar, Hadi] Ardakan Univ, Dept Chem Engn, Fac Engn, POB 184, Ardakan, Iran; [Fallah-Mehrjardi, Mehdi; Behjatmanesh-Ardakani, Reza] Payame Noor Univ, Dept Chem, Tehran 193953697, Iran; [Munawar, Khurram Shahzad] Univ Sargodha, Dept Chem, Punjab, Pakistan; [Munawar, Khurram Shahzad] Univ Mianwali, Dept Chem, Mianwali, Pakistan; [Ashfaq, Muhammad; Tahir, Muhammad Nawaz] Univ Sargodha, Dept Phys, Punjab, Pakistan in 2021.0, Cited 33.0. Category: thiomorpholine. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6

A novel dioxomolybdenum Schiff base complex, MoO2L center dot DMF, was synthesized by treating MoO2(acac)(2) with an ONO donor Schiff base ligand (H2L) derived by the condensation of 4-aminobenzohydrazide and 3-methoxysalicylaldehyde. The synthesized ligand and complex were characterized by physicochemical and spectroscopic techniques. Single-crystal X-ray analysis was also accomplished to ensure the molecular structure of the complex. The geometry around the central metal atom in MoO2L center dot DMF was distorted octahedral as revealed by the data collected from diffraction studies. Theoretical calculations of the synthesized compounds were carried out by DFT at B3LYP/Def2-TZVP level of theory, which showed a good correlation with the experimental findings. Moreover, the homogeneous catalytic efficiency of the complex was investigated by the process of selective oxidation of benzylic alcohols using urea hydrogen peroxide (UHP) in acetonitrile under reflux conditions.

Category: thiomorpholine. Welcome to talk about 99-61-6, If you have any questions, you can contact Kargar, H; Fallah-Mehrjardi, M; Behjatmanesh-Ardakani, R; Munawar, KS; Ashfaq, M; Tahir, MN or send Email.

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Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

An article Catalyst-free UV365-assisted synthesis of pyran annulated heterocyclic scaffolds and evaluation of their antibacterial activities WOS:000586094300001 published article about ONE-POT SYNTHESIS; VISIBLE-LIGHT PHOTOCATALYSIS; PHOTOREDOX CATALYSIS; EFFICIENT SYNTHESIS; ANTIMICROBIAL EVALUATION; MULTICOMPONENT SYNTHESIS; TREATED SOLUTIONS; RAPID SYNTHESIS; DERIVATIVES; ACID in [Dutta, Arup; Rahman, Noimur; Nongkhlaw, Rishanlang] North Eastern Hill Univ, Dept Chem, Shillong, Meghalaya, India; [Kumar, John Elisa] North Eastern Hill Univ, Photocatalysis Lab, Shillong, Meghalaya, India; [Rabha, Jintu; Phukan, Tridip] Gauhati Univ, Dept Bot, Gauhati, Assam, India in 2021.0, Cited 59.0. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6. Computed Properties of C7H5NO3

A convenient and eco-friendly, one-pot synthetic protocol for pharmaceutically important pyran-based heterocyclic compounds is repeated herein. The reactions were carried out at room temperature in a water-ethanol solvent mixture under direct irradiation of UV365 light source in the absence of photocatalyst. The merits of the present protocol include mild and catalyst-free reactions, green procedures, and high yields. The added advantage of this protocol is that it can be applied for large-scale synthesis of various pyran-based heterocyclic compounds without employing any expensive catalyst. Also, in vitro antibacterial screening of pyran derivative was investigated against both Gram-positive Bacillus cereus (B. cereus) and Gram-negative bacteria Escherichia coli (E. coli).

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Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

Zheng, ZB; Han, BB; Hu, JJ; Li, XW in [Zheng, Zubiao; Han, Bingbing; Hu, Junjun; Li, Xianwei] Huangshan Univ, Dept Chem, Huangshan City 245041, Anhui, Peoples R China published Application of Poly(Vinylbenzyltrimethylammonium Tribromide) Resin as an Efficient Polymeric Catalyst in the Acetalization and Diacetylation of Benzaldehydes in 2021.0, Cited 43.0. Application In Synthesis of 3-Nitrobenzaldehyde. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6.

The applications of a new supported tribromide reagent (poly(vinylbenzyltrimethylammonium tribromide) resin) were reported. This supported tribromide resin was used as a catalyst in the acetalization and diacetylation of benzaldehydes under mild conditions with high efficiency. The effects of solvents, and amount of the supported tribromide resin on the reactions were investigated. Under the optimal conditions, most of acetal and 1,1-diacetates of benzaldehydes were selectively obtained in excellent yields.

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Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

Product Details of 99-61-6. In 2021.0 J IRAN CHEM SOC published article about HYBRID MAGNETIC NANOCATALYST; ONE-POT; SILICA NANOPARTICLES; GREEN; PROTOCOL in [Keshavarz, Mahnoush; Nikpassand, Mohammad] Islamic Azad Univ, Fac Basic Sci, Dept Chem, Rasht Branch, POBox 41335-3516, Rasht, Iran; [Mamaghani, Manouchehr] Univ Guilan, Fac Sci, Dept Chem, POB 41335-1914, Rasht, Iran; [Dekamin, Mohammad G.] Iran Univ Sci & Technol, Dept Chem, POB 16846-13114, Tehran, Iran in 2021.0, Cited 37.0. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6.

A heterogeneous organic-inorganic hybrid durable nanocatalyst gamma-Al2O3@Silane-TMG was prepared by covalently functionalization of nano-gamma-Al2O3 through anchored 3-chloropropyl- trimethoxysilane with 1,1,3,3-tetramethylguanidine (TMG). The structure of the catalyst was characterized by various techniques including FT-IR, XRD, SEM, EDX and TGA analyses. The synthesized nanocatalyst was successfully used in an efficient and green four-component synthesis of pyrazolopyranopyrimidine derivatives using ethyl acetoacetate, hydrazine hydrate, arylaldehydes and barbituric acid (or thiobarbituric acid) in H2O at 40 oC. This practical method produced the desired products at reduced reaction times (10-25 min) and high to excellent yields (85-98%). The main advantages of this practical method are the use of heterogeneous basic nanocatalyst, simple work-up procedure with no need to chromatographic purification, affording highly selective conversion and recyclability of the catalyst which could be used in 5 cycles with only a small decrease in its activity. [GRAPHICS] .

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Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

Authors Matamoros, E; Cintas, P; Palacios, JC in ROYAL SOC CHEMISTRY published article about in [Matamoros, Esther; Cintas, Pedro; Palacios, Juan C.] Univ Extremadura, Fac Ciencias, Dept Quim Organ & Inorgan, E-06006 Badajoz, Spain; [Matamoros, Esther; Cintas, Pedro; Palacios, Juan C.] Univ Extremadura, IACYS Unidad Quim Verde & Desarrollo Sosteni, E-06006 Badajoz, Spain in 2021.0, Cited 61.0. Computed Properties of C7H5NO3. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6

Construction of enantiopure carbohydrate conjugates incorporating heterocyclic fragments is often hampered by the necessity of protection/deprotection protocols and multistep routes. Here we show the preparation and structural features of a broad series of chiral 1,3-oxazolines and 1,3-oxazines embedded in a hydrophilic chain based on glycamines, which bypass the disadvantages associated with labile anomeric positions. These substances, however, interconvert in solution and show dynamic equilibria that can be altered by crystallization. A variety of substitution patterns at the heterocyclic moiety disclose the structural and stereochemical relationships. Equilibria monitored by NMR experiments and aided by DFT calculations provide data on kinetic and thermodynamic stability. The reaction proceeds via the intermediacy of iminium ions as a unifying element controlling the steric outcome.

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Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

Recommanded Product: 3-Nitrobenzaldehyde. Authors Rahmatizadeh-Pashaki, Z; Daneshvar, N; Shirini, F in SPRINGER published article about in [Rahmatizadeh-Pashaki, Zahra; Shirini, Farhad] Univ Guilan, Coll Sci, Dept Chem, Rasht 4133519141, Iran; [Daneshvar, Nader] Univ Guilan, Dept Chem, Univ Campus 2, Rasht, Iran in 2021.0, Cited 69.0. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6

In this work, [H-2-Bisim][H2PO4](2) as a novel bis-imidazole-based acidic ionic liquid has been synthesized and characterized with a variety of techniques including FT-IR, H-1, C-13, P-31 NMR and mass spectroscopy techniques. After characterization, this compound was used as an affordable and recyclable catalyst in the synthesis of arylidene malononitrile, ethyl (E)-3-(aryl)-2-cyanoacrylate and tetrahydrobenzo[b]pyran derivatives. The procedure had several advantages such as excellent yields, short reaction times, simple workup and use of a non-expensive and non-toxic compound as the catalyst. Moreover, the prepared ionic liquid could be recycled and reused without significant loss in its catalytic activity in the studied reactions.

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Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem