In 2021.0 ORG LETT published article about FUNCTIONALIZATIONS; DERIVATIVES; METALATION; ALKYNES; ESTERS; ACID; KEY in [Huo, Jiaqi; Yang, Yunhui; Wang, Congyang] Chinese Acad Sci, CAS Res Educ Ctr Excellence Mol Sci, Inst Chem, Beijing Natl Lab Mol Sci,CAS Key Lab Mol Recognit, Beijing 100190, Peoples R China; [Huo, Jiaqi; Yang, Yunhui; Wang, Congyang] Univ Chinese Acad Sci, Beijing 100049, Peoples R China; [Yang, Yunhui; Wang, Congyang] Huairou Natl Comprehens Sci Ctr, Phys Sci Lab, Beijing 101400, Peoples R China in 2021.0, Cited 49.0. The Name is Benzophenone. Through research, I have a further understanding and discovery of 119-61-9. Quality Control of Benzophenone
Stoichiometric cyclomanganation of aromatic ketones and further reactions of the thus-formed manganacycles with isocyanates were first reported by Kaesz and Liebeskind in 1975 and 1990, respectively. The buildup of a closed manganese catalytic cycle for the reaction of ketones and isocyanates remains an unsolved problem. Herein, an unprecedented trio of Me2Zn/ AlCl3/AgOTf is developed to build up manganese catalysis, which enables the [3 + 2] cyclization of ketones with isocyanates via inert C-H activation to access 3-alkylidene phthalimidines in a straightforward manner unachieved by other transition metal catalyses.
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Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem